Document Type
Article
Publication Date
2025
Publication Title
Journal of Chemical Crystallography
Keywords
crown ether, hydrogen bonding, crystal structure, Hirshfeld analysis
Abstract
The compound 1,4,7-trithia-10,13-diazacyclopentadecane-9,14-dione, 1, crystallizes in the space group P21/c with a = 9.3608(3) Å, b = 16.0333(5) Å, c = 9.5608(3) Å, β = 113.3521(14)°, and Z = 4. The title molecule forms chains via face-to-face N–H…O hydrogen bonds. The structure of 1 is also compared to the previously reported oxygen analog, 1,4,7-trioxa-10,13-diazacyclopentadecane-9,14-dione.
Funding Source
This article was published Open Access thanks to a transformative agreement between Milner Library and Springer Nature.
DOI
10.1007/s10870-025-01054-5
Recommended Citation
Jugovic, T.M., Hamaker, C.G. Crystal Structure Analysis of 1, 4, 7-Trithia-10, 13-diazacyclopentadecane-9, 14-dione. J Chem Crystallogr (2025). https://doi.org/10.1007/s10870-025-01054-5
Comments
First published in Journal of Chemical Crystallography (2025): https://doi.org/10.1007/s10870-025-01054-5
Supplemental data attached.
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